Scientific method + Evolution = the perfect juice? (HA!)

So now in this story, it's late November into December. The cruelest time, atmospherically speaking, to bubble. Good. If I can make a formula work in midwinter, surely it would be easily adaptable for fair weather months.

I was young and naive those few months ago. And forgetful.

My game plan: figure out what components are necessary to include in a soap bubble formula. Understand what qualities each one brings to the mix. Gather many variations of each component. Test different brews, in a controlled experiment, recording the results faithfully. Whittle away at the options keeping only the best combinations. The net result would be dishpan hands and the perfect juice. It would be a combination of the scientific method and evolution. It would take some time, but that's okay. Time and patience I have plenty of. The result would be a perfectly engineered bouncing baby bubble (juice) I could call my own.

My efforts I'll outline here, but let me tell you now: I forgot to use distilled water. I used tap water. I should have varied the soap I used and I didn't. I got so caught up in "the length of bubble life has everything to do with the glycerine/viscocity angle" that I neglected to take into account soap and water. Stupid.

Did I still learn a lot about what makes bubbles tick? Sure. But distilled water and a better choice in soap would have resulted in a grander payoff. With that in mind, here's what happened. It was mostly a viscosity/elasticity/antievaporation experiment.

I knew the mix had to contain:
1. Water.
2. A liquid dish detergent.
3. Something to thicken it. Some sites recommended glycerine. Others, a dose of commercial bubble juice. Another site (Bubbletown) suggested increasing viscosity with boiled flax seed water.

1. After investigating the difference between distilled water, spring water and tap water, I discovered distilled water contained far fewer minerals and other elements that might act to reduce the power of the surfactants in the soap/detergent. And then I promptly forgot to use distilled water.
2. Bubblers were either "Dawn" or "Joy" fans and chose concentrate or non concentrated versions of their brand of choice. Joy sounded more promising than Dawn. As if success was already here and I wouldn't have to wait for tomorrow. Non-ultra sounded better because it was cheaper and I was about to burn through a lot of dish soap. So, Joy Non Ultra. (I had so much to learn!)
3. Viscosity. This intrigued me. The more viscous a liquid is (normal people call it "thicker") the longer the juice is supposed to take to drain to the bottom of a bubble. It helps to delay evaporation. It also makes for thicker walled bubbles, and that promotes brighter rainbow colors as well. Longer life and better looking? Like most Americans this aspect caught my eye and seduced me.

Each of the mixes described below was tested against my "control" solutions. Fan Yang Special Solution #1 & #2. Number one, I got from SteveSpanglerScience.com, and from day one it blew my socks off. These days I can brew up batches I like better but Fan's #1 solution was a real eye opener for me. I got it early on and it beat the pants off of Mr. Bubbles who was my long standing hero. #1 lived longer, took harsher punishment, repeatedly bubble in bubbled - Something I couldn't get Mr. B to do in the arid mid winter. Fan's #2 I got from an ebay auction. Same label. Different stuff. Even smelled different. It smelled like Puestefix, if you know what I mean.

#1 lasted twice+ as long as #2. I've since bought more of Fan's Special Solution, but have never found one that plays as well as that first bottle. Anyway, those were my unaltered control solutions. I still haven't figured out why Fan put the same label on what were clearly different solutions. Later, I read on his website that he was marketing certain bottles to the US and others to Canada and that he had some sort of relationship with Pustefix, later with Gazillion. If YOU know (or have an idea about) why these bottles contained different juice, please contact me. Both were bought late in '04.

On to viscosity. I found 2 kinds of glycerine. The cheap kind came off the shelf of a local drug store in a four ounce bottle in the skin care isle. The expensive kind came from behind the counter in a W-Mart pharmacy. The cheap kind was thicker/more viscous. The expensive glycerine was thinner and somehow looked cleaner. Purely opinion, but it did pour less gloppily. This distinction between "expensive" and "cheap" glycerine I found later has to do with manufacture and purity. The expensive glycerine was Kosher grade vegetable glycerine, made from coconut oil mostly. It's the kind of glycerine you can cook with or add to drinks to sweeten them up. The cheap glycerine I believe is a byproduct of soap making process which often includes rendering animal fats or something. It's not toxic but not edible. Less "pure" and of more questionable manufacture/origin. You find it by the gallon in chemical supply houses online. The expensive stuff you find in healthfood/aromatherapy/natural soap making supplies online.

In researching glycerine and viscosity, my mind wandered (after considerable research and a comment from my wife) to
personal lubricants. Those tubes of slippery stuff they sell in the unmentionable dept. of drug stores. Not only did many of them contain glycerine, they had other stuff in them that made them even more viscous (thicker-remember?). I marched right into the unmentionable isle of three different stores and loaded up a basket with Astroglide gel, KY jelly, Brooks brand jelly, Equate which is W-Mart's brand jelly. Months later I found Surgilube at a medical supply store. Surgilube might just be my favorite lube at the moment.

Now, I was all set for a radical binge of soap bubble brewing in my basement.

In retrospect, I should have picked up a hygrometer to keep track of humidity. I also should have bought more Mr. Bubbles to use in the tests but was having trouble finding big bottles of it so I went with Miracle Bubbles as the commercial bubble solution when included in the tests.

Tests: Speaking of the "test", it was what I called a timed "hang" test. Always with the same wand (a Mr. B wand rinsed between tests) I would blow a few bubbles and let them drop to the floor. Then I would re-dip and blow a softball sized bubble, catch it, and hang it off of the edge of the table from an alligator clip/weight which was on the table. I started timing when the bubble was caught. Knocked off big drips with a straw. Recorded the time when the bubble popped. Then re-dipped to make a slightly bigger bubble, released it about face height and tried to blow a bubble through the side for a bubble in a bubble. If it didn't pop, I caught it, brought it back up released it to try it again. So it was a "hang" test and a "bubble in bubble" test.

In many small plastic containers with lids I mixed up these various concoctions in one night. Tested them all for the first time that night and each of two consecutive nights, and recorded these results:

Mix 1. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 3 teaspoons expensive glycerine. First thoughts: Light, could double bubble once but brittle soon after. Added another teaspoon glycerine. Hang test: 2:48. Clean pop. No residue, or what I would later call "beard". At 24 hours, could double bubble easily, not so brittle. 2:04 on hang test. Added 1 teaspoon each glycerine & detergent. 48 hour test: 3:45 on hang test. Could double bubble.

Mix 2. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 3 teaspoons of cheap glycerine. Light. Could almost double bubble. More brittle than #1. Hang test 2:26. No beard. 24 hours: 2:04 hang test, no double bubble. Added 1 teaspoon each cheap glycerine and detergent. Still brittle. 48 hours: 3:30. No double bubble.

Mix 3. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 1 tablespoon Equate. Medium heavy feel, clear. could double bubble 8x. Hang time:2:52. 24 hours: could still double bubble very well. Hang time 1:16. Added 1.5 teaspoon cheap glycerine. No instant change. Added 1 teaspoon detergent. Hang test 1:45.

Mix 4. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 1 tbl brooks jelly (very similar to Equate) More brittle than #3. Could double bubble some. Hang test 2:05. 24 hours: Very excited. Good colors and durable. Hang test 1:22. Added 1/2 teaspoon cheap glycerine to retard evaporation-boosted hang time by over 10 seconds. 48 hours: added 1/2 teaspooon Brooks Jelly. Hang test 1:35.

Mix 5. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 1 tablespoon KY jelly. Medium heavy feel. Double bubble 10 times. Seems to hold interior floating bubbles better than others. Hang test 2:26. Popped with beard. 24 hours: Heavy and durable. Hang test 1:29. Added 1/5 teaspoon expensive glycerine. 48 Hours: still happy. Hang test 1:45 - longer than other jellies, shorter than just glycerine, much more able to double bubble than glycerin recipes.

Mix 6. 1 cup water (tap), 1 tablespoon plus 1 teaspoon detergent (Joy non ultra), 1 tablespoon Astro glide gel. Heavy nice color, could double bubble 10x, doesn't hold interior bubbles as well as mix 5. Popped with beard at 1:55. 24 hours: Not as heavy as mix 5, very durable, a bit more brittle but better looking colors. hang test 1:23. Added 1/2 teaspoon expensive glycerine. 48 hours: 1:45 hang test, plays about the same as mix 5.

Fan Yang #1. hang test 2:46. Clear and smells of dishwashing soap. could double bubble 6x. 24 hour hang test: 2:48 died with beard. 48 hour hang test: 2:40.

Fan Yang #2. Hang test 1:18. Smells of baby powder and is milkier looking than fan yang #1. 24 hours: 1:00. Is it Pustefix? 48 Hours: :55 seconds.

special mixes...

Mix # 7. 1/3 each Miracle bubbles, water, cheap glycerine. Gooey, could not double bubble. Too thick. Hard to blow bubble but it lasted a long time in hang test. 3:51. Died with small beard. 24 hours: could not make bubble. Added 1 tbl. joy detergent and could double bubble immediately and made it fun to play with. Died with beard at 12:00!, Added another tablespoon of joy. Hang test 22:30! 48 hours: 2:56 hang test. This one lived the longest. Did die with beard.

Mix #8. 1 cup of boiled flax seed water (see Bubbletown site), 1 tablespoon and one teaspoon Joy, 2 teaspoons cheap glycerine. Because the flax water is so viscous, it's syrupy, could double bubble 3x, it's makes great looking bubbles as the walls are so thick. Hang test 5:28, died with beard. 24 Hours: Much more brittle. hang test 1:44. So I added 1 teaspoon joy which once again restored it's elasticity and I could double bubble. 48 hours: still very syrupy. Added 2 tbs water and 1 tbs joy. Not so much improvement. hang test 1:45.

Mix #9. 1 cup flax seed water, 1 tablespoon and 1 teaspoon Joy. 1 Tablespoon Astroglide. Thick. Could double bubble easier than #8. Sticky and beard when pops. Hang test 2:12. 24 Hours: Same. Hang test 1:30. Added 1/2 teaspoon expensive glycerine to extend time. Didn't work. 48 Hours: hang test 1:30.

Mix #10. 1 Cup Mr. Bubbles. 1 tablespoon KY. Best of the special solutions. A bit brittle, good colors, holds interior bubbles well, double bubble 8x. hang test 1:55, died with beard. 24 hours: very brittle so I added 1 teaspoon Joy, much less brittle now, so I added 1 teaspoon more Joy. Now water seems to run out of it in a stream down sides. Might need time to incorporate the ingredients. Hang test :57. 48 hours: No change.


With these tests I learned how to observe the bubbles and started to take guesses at what the different amendments might do for the juices, to improve their performance. The personal lubricants surprised me and I went on to work more with them in the mix. I learned that adding just a bit more soap can make a big difference in the qualities of bubbles. I was surprised by that mix number 7 when it jumped from a hang test time of 12:00 to 22:30 with just a tablespoon of Joy and 24 hours making the difference.

I was left wondering if glycerine is an anti evaporation agent, what was it about the expensive glycerine that made it better for the mix? Head to head, the expensive vegetable grade glycerine out performed the cheap glycerine measurably in both longevity and skin elasticity. It was true each time I tested here and when I repeated the tests later in more sophisticated brews.

The personal lubricants I was assuming would simply be another way of introducing glycerine and greater viscosity. Much more than that happened. On closer examination of the lubes, Equate and Brooks Gels had similar ingredient lists which differed from KY and Astroglide Gels which had nearly identical ingredients. There will be more about this in the bubble juice cookbook pages but the gels added a huge double bubble advantage/potential. And although in these tests the KY/Astroglide pair made the bubble skin slightly more supple than the Brooks/Equate pair, I liked Equate the best of them all because it left less of a messy beard at pop time.

I learned that the lube which added flexibility/elasticity also adds weight to the bubble. This would certainly be a factor when deciding which mix to use when making bubble chains for instance. The added weight would pull them apart while a straight glycerine blend would be lighter for longer chains/caterpillers. However, bubbles blown into bubbles floating in the air would be easier to do with the more flexible skin and greater mass/weight of a lube based mix.

In the end I was still up in the air about the role of detergent beyond allowing water to form a film. Why did dish detergent play such an enormous role in allowing mix number seven to increase the hang time? Was it simply reducing the surface tension or did it also delay evaporation? Too much detergent adversely effected mix number 8 at the 48 hour mark.

With these few tests under my belt, it was time to go back to the internet and look at the different bubbler's sites to examine the kinds of work they were doing and the recipes they were recommending.

FYI: The Bubbletown website mentions boiled linseed oil to increase viscosity. After some research and trial and error I found linseed is also flax seed which is available in health food stores. I used a closely woven mesh bag (the kind you use to wash delicate items in the laundry) into which I put a tablespoon of flax seed. I got a pot of water (4 cups) boiling on the stove and set the bag in to boil until the color of the water was amber. I took the pot off the heat. I squeezed the jellied goop out of the bag, through the holes but the physical seed remained inside, strained from the broth. When the flax seed water cooled , it was indeed like a mucus substance. After much experimentation with this flax seed broth, (diluting it, using it straight up, boiling it for shorter and longer durations) it still did not compare with personal lubricants as a way of altering viscosity and elasticity of the mixes I tried. Perhaps you'll get lucky with flax seed. I certainly wanted to. It was way cheaper and seemed to offer much promise but it didn't pan out for me. Too bad. Also, I think because this is unprocessed oil, the brews over time might go rancid. Let me know if you ever make this thickener work.

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